Course code KJM314

KJM314 Applied Organic Analytical Chemistry

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Showing course contents for the educational year starting in 2019 .

Course responsible: Roland Peter Kallenborn
Teachers: Hanne Marie Devle, Dag Ekeberg, Siri Merete Grønhovd, Yngve Henning Stenstrøm, Morten Sørlie, Laura Röhler
ECTS credits: 10
Faculty: Faculty of Chemistry, Biotechnology and Food Science
Teaching language: EN, NO
(NO=norsk, EN=Engelsk)
Limits of class size:
20
Teaching exam periods:
This course starts in the autumn semester This course has teaching/evaluation in the autumn semester .
Course frequency: per year
First time: 2012V
Course contents:

The course will focus on various applications for organic analytical chemistry:

  • HPLC: for purification and isolation of organic compounds
  • GC/MS and GC/ECD: within environmental chemistry and pollution
  • LC/MS, GC/MS and GC/FID: for product control in technical applications and synthesis
  • LC/MS and GC/MS: for purification and product control within drug and food production.

Quantitative standard methods like GC/MS, as well as purification methods like column chromatography and SPE, Silica based, and Alumina-based chromatography will be applied and evaluated. Critical method validation and quality control will be integrated in both lectures and practice.

Learning outcome:
A practical guidance is provided into the analytical organic chemistry as a versatile tool in a variety of applications spanning from technical control, product control to pharmaceutical application, food safety, environmental chemistry and medical/ health related applications.   After completion, the candidates should have knowledge of, and be familiar with, the various analytical techniques used for sample purification and quantitative analysis using a variety of separation and detection techniques, including mass spectrometry, UV-VIS detection etc. Interpretation of chromatograms and quantification procedures are central topics. Students will become familiar with the validation of methods for specific applications and will be able to select appropriate methods for a specific application within the field of organic analytical chemistry.
Learning activities:
There will be lectures and seminars where students are expected to be involved in a constructive and active way. Students are given a project to work on and present in plenary. Laboratory experiments were laboratoryreports must be handed in and will be evaluated before the written exam. 
Teaching support:

Office hours will be announced. Seminars will be held in which the laboratory work is discussed. 

Canvas.

Syllabus:
Lecture printouts as well as selected scientific publications.
Prerequisites:
The course is based on scientific knowledge in generell Chromatography (KJM310) and Mass Spectrometry (KJM313) (both may be taken in parallel).
Recommended prerequisites:
A good understanding of the general principles and methods in organic analytical chemistry is a prerequisite for the successful completion of the course.
Mandatory activity:
Participation in colloquiaParticipation in course seminarsExperimental assignments
Assessment:

3 hours written exam, counts 60 %

Written report, counts 40 %

Nominal workload:
Lectures: 52 hours. Practical exercises: 78 hours. Individual study: 170 hours (including project work).
Entrance requirements:
Special requirements in Science
Type of course:
4 hours with lectures/ seminars and 6 hours with laboratory exercises per week.
Examiner:
An external examiner approves the examination questions and marks a minimum of 25 randomly selected examination papers.
Allowed examination aids: C2 Alle typer kalkulatorer, alle andre skriftlige hjelpemidler.
Examination details: Continuous exam: A - E / Ikke bestått